https://doi.org/10.1039/D2TA02897B “To obtain a full 3D representation of the formed MgCO3 crystal, we performed additional focused ion beam (FIB) SEM tomography measurement of MgCO3 grown on MgO(100)
https://doi.org/10.1039/D2TA02897B “We gained further insight into the morphology and location of formation of MgCO3 that is formed during carbonation by SEM (Fig. 5 and S6–S8†). Prior to
https://doi.org/10.1039/D2TA02897B “Subsequently we used plasma FIB-SEM to obtain a smooth cross-section of a groove allowing for high quality stacks of SEM images of cross-sections through
https://doi.org/10.1039/D2TA02897B “The location of MgCO3 formed in the NaNO3–MgO model systems after their exposure to CO2 is identified by Raman micro-spectroscopy, SEM energy dispersive X-ray spectroscopy (EDX),
https://doi.org/10.1039/D2TA02897B “To visualize and quantify the volume of NaNO3 in the grooves of the model samples after CO2 capture we turned to X-ray micro computed tomography (μCT), Fig.
https://doi.org/10.1039/D2TA02897B “To visualize and quantify the volume of the magnesium carbonate formed through CO2 absorption at the bottom of the grooves in the NaNO3–MgO_B model system,
https://doi.org/10.1039/D2TA02897B “The fabrication of the NaNO3–MgO model structure is illustrated in Fig. 1. We used ultra-short pulse (USP) laser ablation to microstructure MgO(100) single crystals with
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